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#1
Start by
Albadr Alahdal
03-26-2014 12:10 PM

Agitated pressure filter dryer

Hi, I'm doing a design project for the agitated filter dryer, also known as pressure filter dryer. I was just wondering if any of you gentlemen can help me with that, I'm mainly looking for the chemical principle associated with this unit. Thank you!
03-26-2014 02:28 PM
Top #2
Kieran Nurmi
03-26-2014 02:28 PM
Are you referring to pressure nutsche filtration? If so, this might help; http://onlinelibrary.wiley.com/doi/10.1002/prs.680180308/abstract

While I don't have any experience, I would suggest looking it up in a drying techniques textbook. Your university library probably has something suitable, but for out of hours access, you might be able to find something in the Knovel library through IChemE.
03-26-2014 05:18 PM
Top #3
Horwath Jim
03-26-2014 05:18 PM
Google for manufacturer web sites. These should have info or application case studies.
03-26-2014 07:24 PM
Top #4
Albadr Alahdal
03-26-2014 07:24 PM
Thank you all for your kind comments. Kieran, im sorry yes i did mean the pressure nutsche filtration, Thanks alot!
03-26-2014 10:17 PM
Top #5
Ian Kemp
03-26-2014 10:17 PM
A pressure filter dryer can basically be treated as a batch contact (conduction) dryer for the drying stage. Basic calculation methods can be found in Perry's Chemical Engineers Handbook, Coulson and Richardson and other standard texts - probably adequate for what you need. Likewise the filtration stage can be calculated as a standard pressure filtration.
03-27-2014 12:23 AM
Top #6
Horwath Jim
03-27-2014 12:23 AM
There is typically a hot nitrogen flow thru the solids, which are agitated, during the drying phase.
03-27-2014 02:41 AM
Top #7
Ian Kemp
03-27-2014 02:41 AM
Or, to put Jim's comment another way - there should be a hot nitrogen flow if the dryer was designed or specified by good process engineers. But I have seen a surprising number of filter dryers just working with cold nitrogen on blowdown and drying, and saddling the users with much longer drying times as a result.

Hot nitrogen should theoretically be better for the blowdown phase as well, as the surface tension of the liquid is reduced and it dewaters more easily to a lower moisture content, thus saving significant energy. However, I'm not sure how widely this is used. In paper drying, which is of course very energy intensive, huge savings were made by heating the first few rollers.
03-27-2014 05:36 AM
Top #8
Horwath Jim
03-27-2014 05:36 AM
The Filter Dryers are not necessarily used to produce a dry or wet cake. the separated solids can be reslurried and transferred to a subsequent vessel for further processing. If the wet cake can be reslurried without final removal of solvent this is a an additional energy savings to help justify the expensive filter dryer unit.
03-27-2014 07:41 AM
Top #9
Albadr Alahdal
03-27-2014 07:41 AM
Thank you all for the comments, really appreciate it! Well the Filter Dryer process I'm designing, is first to strip/filter out the mother liquor with all the unwanted solvents out leaving behind the product ("R-flurbiprofen" that's what i'm after), then drying it and finally as Horwath mentioned reslurring the cake with toluene. The problem i'm having is finding the right dimensions for the unit. But now i'll follow what Ian said, and see how it goes. Again thanks alot for the help everyone!!!
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